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dc.contributor.author | AVILA HERNANDEZ, MARCO ANTONIO | |
dc.contributor.author | PEREZ ALONSO, CESAR | |
dc.contributor.author | OROZCO VILLAFUERTE, JUAN | |
dc.contributor.author | BARRERA DIAZ, CARLOS EDUARDO | |
dc.contributor.author | ALPIZAR REYES, ERIK | |
dc.contributor.author | CRUZ OLIVARES, JULIAN | |
dc.creator | AVILA HERNANDEZ, MARCO ANTONIO; 860124 | |
dc.creator | PEREZ ALONSO, CESAR; 122909 | |
dc.creator | OROZCO VILLAFUERTE, JUAN; 84355 | |
dc.creator | BARRERA DIAZ, CARLOS EDUARDO; 25379 | |
dc.creator | ALPIZAR REYES, ERIK; 628114 | |
dc.creator | CRUZ OLIVARES, JULIAN; 69160 | |
dc.date.accessioned | 2022-10-01T02:25:09Z | |
dc.date.available | 2022-10-01T02:25:09Z | |
dc.date.issued | 2022-08-02 | |
dc.identifier.issn | 0100-4042 | |
dc.identifier.uri | http://hdl.handle.net/20.500.11799/136414 | |
dc.description | Anthocyanins from LSB and with a PEF pretreatment were extracted with ethanol + SCCO2. The extraction at 200 bar, 333.15, 3.3% wt. of ethanol as cosolvent and using LSB with a PEF pretreatment of 1 kV/cm, produced an extraction yield of 0.284 % and a TAC of 0.231 (g/100 g of ethanol + SCCO2). The individual effect of 1.0 kV/cm of PEF pretreatment increases the %EY by 25 % and the TAC by 29 %. The individual effect of the cosolvent increases the %EY by 32% and that of TAC by 36.4%. However, the combined effect of 1.0 kV cm-1 and 3.3 % ethanol, produced an increase of 78.2 % and 85.3% in the %EY and TAC, respectively. Therefore, these results suggest that there is a synergistic effect, which means that both the electroporation caused by PEF in the LSB and the increase in polarity due to the addition of ethanol produce a substantial improvement over %ET and TAC. Furthermore, the process of extracting anthocyanins from LSB using a mixture of ethanol + supercritical carbon dioxide can be satisfactorily described by a solubility-based model such as the Kumar and Johnston model. | es |
dc.description.abstract | The lyophilized strawberry anthocyanins were extracted using a supercritical extraction (SE) process. The effect of pulsed electric fields (PEF) as pretreatment and the influence of the addition of ethanol as a cosolvent on the percentage of extraction yield (EY) and the total anthocyanin concentration (TAC) were analyzed. The effect of PEF was evaluated at 0.5 and 1.0 kV/cm, while the effect of the cosolvent was studied in mixtures of supercritical carbon dioxide - ethanol (SCCO2 + ethanol) at 1.6 and 3.3% by weight. The best results (% EY = 0.506, TAC = 0.428 g /100 g of lyophilized strawberry) were obtained with a PEF pretreatment of 1.0 kV cm-1, 3.3%wt. ethanol at 200 bar and 333.15 K. The experimental results of solubility were suitably adjusted with the Kumar and Johnston model. The maximum solubility (0.114 g/100 g of solvent mixture) was obtained at 300 bar and 313.15 K. | es |
dc.description.sponsorship | The authors would like to thank the National Council of Science and Technology of Mexico (CONACyT) for the scholarship granted to the master’s student in chemical sciences Marco A. Ávila-Hernández. | es |
dc.language.iso | eng | es |
dc.publisher | QUIMICA NOVA | es |
dc.rights | openAccess | es |
dc.rights | openAccess | |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0 | |
dc.subject | Lyophilized strawberry | es |
dc.subject | Anthocyanins | es |
dc.subject | Supercritical extraction | es |
dc.subject | Pulsed electric fields | es |
dc.subject | supercritical carbon dioxide | es |
dc.subject | Lyophilized strawberry | |
dc.subject | Anthocyanins | |
dc.subject | Supercritical extraction | |
dc.subject | Pulsed electric fields | |
dc.subject | supercritical carbon dioxide | |
dc.subject.classification | INGENIERÍA Y TECNOLOGÍA | es |
dc.subject.classification | INGENIERÍA Y TECNOLOGÍA | |
dc.title | Supercritical extraction of lyophilized strawberry anthocyanins with pulsed electric fields pretreatment | es |
dc.type | Artículo | es |
dc.provenance | Científica | es |
dc.road | Dorada | es |
dc.road | Dorada | |
dc.organismo | Química | es |
dc.ambito | Internacional | es |
dc.cve.CenCos | 20401 | es |
dc.audience | students | |
dc.audience | researchers | |
dc.type.conacyt | article | |
dc.identificator | 7 | |
dc.relation.doi | http://dx.doi.org/10.21577/0100-4042.20170849 |